Phosphorus-31 NMR: principles and applications
Gespeichert in:
| Weitere Verfasser: | |
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| Format: | Buch |
| Sprache: | English |
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New York [u.a.]
Academic Press
1984
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| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | X, 604 S. |
Internformat
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Datensatz im Suchindex
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| adam_text | PHOSPHORUS-31 NMR PNNCIPLES AND APPLICATIONS EDITED BY DAVID G.
GORENSTEIN DEPARTMENT OF CHEMISTRY UNIVERSITY OF ILLINOIS AT CHICAGO
CHICAGO, ILLINOIS @ ACADEMIC PRESS, INC. HARCOURT BRACE JOVANOVICH,
PUBLISHERS ORLANDO SAN DIEGO NEW YORK AUSTIN BOSTON LONDON SYDNEY TOKYO
TORONTO CONTENTS CONTRIBUTORS XI PREFACE XIII INTRODUCTION DAVID G.
GORENSTEIN TEXT 1 REFERENCES 3 PART 1. PHOSPHORUS-31 CHEMICAL SHIFTS AND
SPIN-SPIN COUPLING CONSTANTS: PRINCIPLES AND EMPIRICAL OBSERVATIONS 1.
PHOSPHORUS-31 CHEMICAL SHIFTS: PRINCIPLES AND EMPIRICAL OBSERVATIONS
DAVID G. GORENSTEIN I. INTRODUCTION AND BASIC PRINCIPLES 7 II.
APPLICATIONS OF 3, P CHEMICAL-SHIFT THEORY AND EMPIRICAL OBSERVATIONS 9
REFERENCES 33 2. PHOSPHORUS-31 SPIN-SPIN COUPLING CONSTANTS: PRINCIPLES
AND APPLICATIONS DAVID G. GORENSTEIN I. INTRODUCTION 37 II. DIRECTLY
BONDED COUPLING CONSTANTS: 7 PX 38 III. TWO-BOND COUPLING CONSTANTS: 2
J PX 42 IV. THREE-BOND COUPLING CONSTANTS: 3 J PX 43 REFERENCES 51 V
PART 2. THEORY AND APPLICATIONS OF PHOSPHORUS-31 NMR TO BIOCHEMISTRY 3.
PHOSPHORAS-31 NMR OF ENZYME COMPLEXES B. D. NAGESWARA RAO I.
INTRODUCTION 57 II. THEORETICAL AND EXPERIMENTAL CONSIDERATIONS 59 III.
EXPERIMENTAL STUDIES OF SPECIFIC ENZYME SYSTEMS 69 IV. COMPUTER
CALCULATION OF NMR LINE SHAPES UNDER THE INFLUENCE OF EXCHANGE 96 V.
CONCLUSION 100 REFERENCES 102 4. 31 P-NMR STUDIES OF PHOSPHOPROTEINS
HANS J. VOGEL I. INTRODUCTION 105 II. CLASSIFICATION OF PHOSPHOPROTEINS
106 III. THEORETICAL AND EXPERIMENTAL CONSIDERATIONS 113 IV. NMR STUDIES
123 V. CONCLUSIONS 144 REFERENCES 149 5. PARAMAGNETIC PROBES OF ENZYME
COMPLEXES WITH PHOSPHORUS-CONTAINING COMPOUNDS JOSEPH J. VILLAFRANCA I.
INTRODUCTION 155 II. GENERAL CONSIDERATIONS 156 III. PROPERTIES OF
CR(III)- AND CO(III)-NUCLEOTIDE COMPLEXES 157 IV. STUDIES WITH
CO(III)-NUCLEOTIDE COMPLEXES 160 V. STUDIES WITH CR(III)-NUCLEOTIDE
COMPLEXES 166 VI. STUDIES WITH CR(III)- AND CO(III)-PYROPHOSPHATE
COMPLEXES REFERENCES 173 6. USE OF CHIRAL THIOPHOSPHATES AND THE
STEREOCHEMISTRY OF ENZYMATIC PHOSPHORYL TRANSFER MING-DAW TSAI I.
STEREOCHEMICAL PROBLEMS STUDIED WITH PHOSPHOROTHIOATES 175 II. 18 0
ISOTOPE SHIFTS IN 31 P NMR 178 III. 17 0 QUADRUPOLAR EFFECTS IN 31 P NMR
181 IV. PROCHIRAL CENTERS: 31 P NMR 185 V. PRO-PROCHIRAL CENTERS: 31 P(
18 0) NMR OR 31 P( N O) NMR 187 VI. PRO-PRO-PROCHIRAL CENTERS: 31 P( 18
0) NMR AND 31 P( 17 0) NMR REFERENCES 196 7. USE OF CHIRAL [ 16 0, 17 0,
18 0]PHOSPHATE ESTERS TO DETERMINE THE STEREOCHEMICAL COURSE OF
ENZYMATIC PHOSPHORYL TRANSFER REACTIONS JOHN A. GERLT I. INTRODUCTION
199 II. SYNTHESES OF OXYGEN CHIRAL PHOSPHATE ESTERS 201 III.
CONFIGURATIONAL ANALYSES OF OXYGEN CHIRAL PHOSPHATE ESTERS 210 IV.
SELECTED EXAMPLES 220 V. SUMMARY 230 REFERENCES 230 8. DNA AND RNA
CONFORMATIONS CHI-WAN CHEN AND JACK S. COHEN I. INTRODUCTION 233 II.
HELIX-COIL TRANSITIONS 234 III. SEQUENCE DEPENDENCE OF DOUBLE-STRANDED
DNA CONFORMATIONS 239 IV. CONFORMATIONAL TRANSITIONS OF DOUBLE-STRANDED
DNA 253 V. DYNAMIC BEHAVIOR OF RNA AND DNA 255 VI. NUCLEOSOMAL DNA 256
VII. BIOLOGICAL AND GENETIC SIGNIFICANCE 259 REFERENCES 260 9.
HIGH-RESOLUTION 31 P-NMR SPECTROSCOPY OF TRANSFER RIBONUCLEIC ACIDS
DAVID G. GORENSTEIN I. INTRODUCTION 265 II. SPECTRAL COMPARISON OF
DIFFERENT ACCEPTOR TRNAS 268 III. MG 2+ DEPENDENCE OF 31 P SPECTRA OF
TRNA PHE 276 IV. MN 2+ EFFECTS ON 31 P SPECTRA OF TRNA* 280 V.
ASSIGNMENT OF 31 P SIGNALS 281 VI. CONFORMATIONAL TRANSITIONS 287 VII.
SPERMINE EFFECTS 291 VIII. 31 P NMR OF YEAST TRNA * E. COLI TRNA*
COMPLEX: SPECTRAL CHANGES 292 IX. CONCLUSIONS 294 REFERENCES 295 10.
PHOSPHORUS-31 NMR OF DRUG-NUCLEIC ACID COMPLEXES DAVID G. GORENSTEIN AND
EVELYN M. GOLDFIELD I. INTRODUCTION 299 II. DRUG-DOUBLE-HELICAL NUCLEIC
ACID COMPLEXES: INTERCALATION 300 III. ELECTROSTATIC MODE OF INTERACTION
310 IV. TRN A-ETHIDIUM 3 P SPECTRA 311 REFERENCES 315 VIII CONTENTS
11. PHOSPHORUS RELAXATION METHODS: CONFORMATION AND DYNAMICS OF NUCLEIC
ACIDS AND PHOSPHOPROTEINS PHILLIP A. HART I. INTRODUCTION 317 II.
GENERAL CONSIDERATIONS 319 III. THE PHOSPHORUS-PROTON NUCLEAR OVERHAUSER
EFFECT 322 IV. PHOSPHORUS RELAXATION TIMES 328 V. SUMMARY 344 REFERENCES
345 12. RELAXATION BEHAVIOR OF NUCLEIC ACIDS: DYNAMICS AND STRUCTURE
THOMAS L. JAMES I. INTRODUCTION 349 II. THEORY 350 III. STRUCTURE AND
POSSIBLE MOLECULAR MOTIONS IN NUCLEIC ACIDS IV. CONSIDERATIONS FOR
NUCLEIC ACID DYNAMICS AND STRUCTURE V. RELAXATION STUDIES OF NUCLEIC
ACIDS 377 REFERENCES 398 13. SOLID-STATE PHOSPHORUS-31 NMR: THEORY AND
APPLICATION TO NUCLEIC ACIDS HEISABURO SHINDO I. INTRODUCTION 401 II.
BASIC CONCEPTS OF SOLID-STATE 3I P NMR 402 III. STUDIES OF ORIENTED DNA
FIBERS 408 IV. STUDIES OF DNA COMPLEXES 418 V. CONCLUDING REMARKS 421
REFERENCES 421 14. PHOSPHORUS-31 NMR OF PHOSPHOLIPIDS IN MICELLES EDWARD
A. DENNIS AND ANDREAS PLUECKTHUN I. INTRODUCTION AND PERSPECTIVE 423 II.
SPECTRAL CHARACTERISTICS OF PHOSPHOLIPIDS IN MIXED MICELLES WITH
DETERGENTS 425 III. 7 I, NUCLEAR OVERHAUSER EFFECT, AND QUANTITATIVE
ANALYSIS 431 IV. SOLUBILIZATION OF PHOSPHOLIPIDS BY DETERGENTS 433 V.
CRITICAL MICELLE CONCENTRATION DETERMINATIONS AND MICELLIZATION OF
MONOMERIC PHOSPHOLIPIDS BY DETERGENTS 435 VI. LYSOPHOSPHOLIPIDS: ACYL
AND PHOSPHORYL MIGRATION 438 VII. PHOSPHOLIPASES: SPECIFICITY AND
KINETICS 442 REFERENCES 444 368 373 CONTENTS IX 15. PHOSPHORUS-31 NMR OF
PHOSPHOLIPIDS IN MEMBRANES LAN C. P. SMITH AND IRENA H. EKIEL I.
PROPERTIES OF MEMBRANES 447 II. 3I P-NMR SPECTRA OF ORDERED SYSTEMS 449
III. OBTAINING 31 P-NMR SPECTRA 457 IV. APPLICATIONS TO BIOMEMBRANES 461
V. CONCLUSION 472 REFERENCES 472 PART 3. APPLICATION TO BIOLOGY AND
MEDICINE: FUTURE DIRECTIONS 16. TWO-DIMENSIONAL PHOSPHORUS-31 NMR
WILLIAM C. HUTTON I. INTRODUCTION 479 II. GENERAL PRINCIPLES OF
TWO-DIMENSIONAL NMR: THE HOMONUCLEAR, J-CORRELATED EXPERIMENT 484 III.
APPLICATIONS OF TWO-DIMENSIONAL SPECTROSCOPY TO 3I P NMR 492 IV.
CONCLUDING REMARKS 509 REFERENCES 510 17. IDENTIFICATION OF DISEASED
STATES BY PHOSPHORUS-31 NMR MICHAEL BAERAENY AND THOMAS GLONEK I.
INTRODUCTION 512 II. SKELETAL MUSCLE 513 III. HEART 530 IV. KIDNEY 533
V. BRAIN 534 VI. EYE 537 VII. MAMMALIAN FLUIDS 540 VIII. PERSPECTIVES
543 REFERENCES 544 PART 4. SELECTED DATA 18. APPENDIXES: SELECTED
COMPILATION OF 31 P-NMR DATA DAVID G. GORENSTEIN AND DINESH O. SHAH
APPENDIX I. DOUBLY CONNECTED PHOSPHORUS (PC) 550 APPENDIX II. TRIPLY
CONNECTED PHOSPHORUS (PO 551 APPENDIX III. QUADRUPLY CONNECTED
PHOSPHORUS (^PC) 563 X CONTENTS APPENDIX IV. QUINTUPLY CONNECTED
PHOSPHORUS (^PC) 586 APPENDIX V. SEXTUPLY CONNECTED PHOSPHORUS (^P^R)
588 REFERENCES 589 INDEX 593
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| spelling | Phosphorus-31 NMR principles and applications ed. by David G. Gorenstein New York [u.a.] Academic Press 1984 X, 604 S. txt rdacontent n rdamedia nc rdacarrier Phosphor-31-NMR-Spektroskopie (DE-588)4137508-7 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 gnd rswk-swf Phosphor (DE-588)4045855-6 gnd rswk-swf Phosphororganische Verbindungen (DE-588)4076094-7 gnd rswk-swf Phosphor-31-NMR-Spektroskopie (DE-588)4137508-7 s DE-604 Phosphororganische Verbindungen (DE-588)4076094-7 s NMR-Spektroskopie (DE-588)4075421-2 s Phosphor (DE-588)4045855-6 s Gorenstein, David G. edt GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=019801959&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Phosphorus-31 NMR principles and applications Phosphor-31-NMR-Spektroskopie (DE-588)4137508-7 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Phosphor (DE-588)4045855-6 gnd Phosphororganische Verbindungen (DE-588)4076094-7 gnd |
| subject_GND | (DE-588)4137508-7 (DE-588)4075421-2 (DE-588)4045855-6 (DE-588)4076094-7 |
| title | Phosphorus-31 NMR principles and applications |
| title_auth | Phosphorus-31 NMR principles and applications |
| title_exact_search | Phosphorus-31 NMR principles and applications |
| title_full | Phosphorus-31 NMR principles and applications ed. by David G. Gorenstein |
| title_fullStr | Phosphorus-31 NMR principles and applications ed. by David G. Gorenstein |
| title_full_unstemmed | Phosphorus-31 NMR principles and applications ed. by David G. Gorenstein |
| title_short | Phosphorus-31 NMR |
| title_sort | phosphorus 31 nmr principles and applications |
| title_sub | principles and applications |
| topic | Phosphor-31-NMR-Spektroskopie (DE-588)4137508-7 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Phosphor (DE-588)4045855-6 gnd Phosphororganische Verbindungen (DE-588)4076094-7 gnd |
| topic_facet | Phosphor-31-NMR-Spektroskopie NMR-Spektroskopie Phosphor Phosphororganische Verbindungen |
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