Verfügbarkeit: Procedures in scanning probe microscopies

Procedures in scanning probe microscopies:

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Bibliographische Detailangaben
Weitere Verfasser:	Colton, Richard J. (HerausgeberIn)
Format:	Buch
Sprache:	English
Veröffentlicht:	Chichester [u.a.] Wiley 1998
Schlagworte:	Scanning probe microscopy Rastersondenmikroskopie
Online-Zugang:	Inhaltsverzeichnis
Beschreibung:	XXXI, 639 S. Ill., graph. Darst.
ISBN:	047195912X

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Datensatz im Suchindex

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adam_text	CONTENTS Preface xvii Editorial Board xix List of Contributors xxi Part 1: Instrumentation (Part Editor: R. Guckenberger, W. Heckl) 1 Introduction 1 Chapter 1.1: Common Techniques and Problems in Scanning Probe Microscopies. 3 Module 1.1.1: Technical Tools 3 Procedure: Piezoelectric Actuators for Scanning Probe Microscopy 3 Module 1.1.2: Test Structures and Calibration 9 Introduction 9 Procedure: Latex Projection Patterns 10 Procedure: Test Sample Structured by Metal Shadowing using Salt Crystals as Mask 12 Procedure: Pt/C Coated Tobacco Mosaic Virus on Glass as a Specimen for Testing SPM Tips 17 Module 1.1.3: Image Processing, Evaluation and Presentation. ... 22 Introduction 22 Procedure: Basics of Fourier Transformation, Convolution and Correlation 24 Procedure: Correction of Specimen Tilt and Line Flattening . 32 Procedure: Real Space Filtering 34 Procedure: Fourier Filtering 37 Procedure: Averaging of SPM Images 40 Procedure: Resolution Assessment 44 Module 1.1.4: Well Known Artifacts Chapter 1.2: STM 50 Module 1.2.1: STM Designs Module 1.2.2: STM Signals and Imaging Modes (Including STM Variants) 50 Introduction 50 Procedure: Conventional Imaging Modes 52 Procedure: Scanning Thermopower Microscopy: a Technique for Organic and Biological Molecules Complementary to STM 55 Procedure: Light Measurements 61 Module 1.2.3: Tips 65 Contents vi Introduction 65 Procedure: Overview of Electro Chemical Tip Etching Methods 67 Procedure: Electro Chemical Etching of Au Tips 69 Procedure: Electro Chemical Etching of Ni Tips 73 Procedure: Manufacturing of W Tips 76 Procedure: Electro Chemical Etching of Au Coated W Tips . 78 Procedure: Electro Chemical Etching of Platinum Iridium and Iridium Tips 81 Chapter 1.3: Atomic Force Microsocopy 85 (Chapter Editor: W. Heckl and O. Marti) Introduction 85 Module 1.3.1: AFM Designs 86 Procedure: Ultrahigh Vacuum Scanning Force Microscopy (UHV AFM) 86 Procedure: Design Principles of Fluid Cells 94 Procedure: AFM and Patch Clamp Technique 98 Module 1.3.2: AFM Signals and Imaging Modes 105 Procedure: Conventional Imaging 105 Procedure: Force Curves in Atomic Force Microscopy ... 110 Procedure: Tapping Mode in Liquids 113 Procedure: Friction and Lateral Forces 116 Module 1.3.3: Force Sensing Elements and Tips 122 Procedure: Bouncing Beam Detection 122 Procedure: Use of the High Linearity Position Sensing Detector in Local AFM Force Measurements 129 Procedure: Force Calibration 133 Procedure: Laser Diode Detection 139 Module 1.3.4: Test Samples 146 Procedure: Preparation of a Compact Disk as a Calibration Sample for AFM 146 Chapter 1.4: Scanning Near field Optical Microscopies Chapter 1.5: Scanning Electro Chemical Methods (Chapter Editor: A. Gewirth) Part 2: Substrates (Part Editor: W. Heckl) 149 Chapter 2.1: General Requirements for Substrates 151 Introduction 151 Chapter 2.2: Conducting Substrates 153 Module 2.2.1: Graphite 153 Procedure: STM and AFM Imaging of Natural Graphite Crystals and Highly Oriented Pyrolytic Graphite (HOPG) . 153 Contents vii Module 2.2.2: Transition Metal Dichalcogenides 156 Introduction 156 Procedure: Molybdenite 158 Procedure: Tungstenite 160 Procedure: Hafnium Disulfide 161 Procedure: Tantalum Disulfide 162 Procedure: Lattice Resolution Imaging of the Layered Dichalcogenide WSe2 by Atomic Force Microscopy and Lateral Force Microscopy 164 Module 2.2.3: Thin Film Metal Layers 167 Procedure: Platinum Carbon, Pt C 167 Procedure: Silver Films 168 Module 2.2.4: Ultraflat Au Surfaces 169 Introduction 169 Procedure: Preparation of Template Stripped Gold (TSG) . . 170 Chapter 2.3: Insulating Substrates 176 Module 2.3.1: Mica 176 Module 2.3.2: Glass as a Substrate for Atomic Force Microscopy Studies 180 Introduction 180 Module 2.3.3: Atomic Force Microscopy of Ionic Crystals 183 Procedure: AFM Imaging of Ionic Crystals 184 Chapter 2.4: Chemically Modified Substrates: Derivatized Surfaces 189 Module 2.4.1: Derivatized Silicon Oxide Surfaces 190 Procedure: Silanization, Imaging, and Patterning of Derivatized Silicon Oxide Surfaces 190 Part 3: Inorganic Systems (Part Editor: B. Parkinson) 201 Introduction 202 Chapter 3.1: Elements 203 Module 3.1.1: Non metallic Elements Module 3.1.2: Coinage Metals 203 Module 3.1.3: Transition Metals Chapter 3.2: Oxides 204 Module 3.2.1: Binary Transition Metal Oxides 204 Procedure: STM Imaging of T O2 X( 110) 204 Procedure: STM Imaging of V2O5 (001) 207 Procedure: STM Imaging of Mo,8O52 (100) 210 Module 3.2.2: Binary Main Group Oxides 213 Procedure: STM Imaging of Conducting Metal Oxide Superlattices 213 Module 3.2.3: Ternary Oxides 219 Contents viii Procedure: STM Imaging of Conducting Molybdenum Oxide Bronzes 219 Procedure: STM Imaging of Rbi/3WO3(0001) 222 Procedure: STM Imaging of Nao.82W03(001) 224 Procedure: STM Imaging of Transition Metal Oxides: SrTiO3 227 Module 3.2.4: Quaternary Oxides (HiTc supercon) Chapter 3.3: Chalcogenides 230 Module 3.3.1: Binary Main Group Chalcogenides InSePbS (Galena). Module 3.3.2: Binary Transition Metal Chalcogenides 230 Procedure: STM Imaging of Layered Structure Metal Dichalcogenides 230 Procedure: STM and AFM Imaging of Zinc Sulfide Nanoclusters 239 Module 3.3.3: Ternary Chalcogenides 243 Procedure: AFM Imaging of Pure and Intercalated Lamellar MPS3 Compounds (M = Mn, Cd, Fe, Ni) 243 Chapter 3.4: Pnictides Module 3.4.1: Main Group Pnictides Module 3.4.2: Transition Metal Pnictides Chapter 3.5: Halides Module 3.5.1: Main Group Halides Module 3.5.2: Transition Metal Halides Module 3.5.3: Alkali Metal and Alkali Earth Halides Module 3.5.4: Ternary Halides Chapter 3.6: Carbides, Silicides and Borides Module 3.6.1: Transition Metal Silicides Chapter 3.7: Intermetallics and Alloys Part 4: Electrochemistry (Part Editor: A. Gewirth) 247 Introduction 248 Chapter 4.1: Electrochemical Surface Preparation Module 4.1.1: Au Surfaces Module 4.1.2: Ag Surfaces Module 4.1.3: Cu Surfaces Module 4.1.4: Pt Surfaces Module 4.1.5: Other Noble Metal Surfaces Module 4.1.6: Semiconductors Module 4.1.7: Other Materials Contents ix Chapter 4.2: Underpotential Deposition 251 Module 4.2.1: Cu Underpotential Deposition Module 4.2.2: Bismuth Underpotential Deposition 251 Procedure: AFM of Underpotentially Deposited Bi on Au(l 11) 251 Module 4.2.3: Pb Underpotential Deposition Module 4.2.4: Tl Underpotential Deposition Module 4.2.5: Cd Underpotential Deposition Module 4.2.6: Ag Underpotential Deposition Chapter 4.3: Halides Module 4.3.1: I on Au(ijk) Module 4.3.2: Br and Cl on Au(ijk) Module 4.3.2:1 on Pt(ijk) Module 4.3.4: Br and Cl on Pt(ijk) Module 4.3.5: I on Ag(ijk) Module 4.3.6: Br and Cl on Ag(ijk) Module 4.3.7: Halides on other Surfaces Chapter 4.4: Organics 257 Module 4.4.1: Oxygen Donors on Au 257 Procedure: Electropolymerization and STM Imaging of Electrically Conductive Polymer Thin Films 257 Module 4.4.2: Sulfur Donors on Au Module 4.4.3: Nitrogen Donors on Au 262 Procedure: STM and AFM Imaging of DNA Bases in Aqueous Solutions under Controlled Potential 262 Module 4.4.4: CO, CN, and SCN on Pt Module 4.4.4: Organic Molecules on Pt/I Surfaces Module 4.4.5: Organics on Cu Surfaces Module 4.4.6: Organics on Ag Surfaces Chapter 4.5: Oxides and Oxidation Module 4.5.1: Oxidation of Au(ijk) Module 4.5.2: Oxide Formation on Cu Module 4.5.3: Oxide Formation on Fe Module 4.5.4: Oxide Formation on Ni Chapter 4.6: Inorganic Overlayers Module 4.6.1: Silicotungstates Chapter 4.7: Semiconductors Module 4.7.1: Si Module 4.7.2: GaAs Module 4.7.3: Ge Module 4.7.4: High Band gap Semiconductors Chapter 4.8: Corrosion of Metals Module 4.8.1: Cu Contents x Module 4.8.2: Fe Module 4.8.3: Steel Module 4.8.4: Al Chapter 4.9: Bulk Deposition of Metals 267 Module 4.9.1: Cu 267 Procedure: In situ SPM Imaging of Bulk Copper Electrodeposition 267 Module 4.9.2: Ni Module 4.9.3: Pb, Cd, Hg Module 4.9.4: Ag 273 Procedure: STM Directed Electro Chemical Deposition of Metal Nanostructures 273 Part 5: Organic Systems (Part Editor: J. Frommer, W. Heckl) . 277 Chapter 5.1: General Considerations 279 Introduction 279 Chapter 5.2: Free Standing Crystals 281 Module 5.2.1: Atomic Force Microscopy of Organic Crystals. . . . 281 Procedure: AFM Imaging of Organic Crystals Materials Selection 282 Procedure: Amino Acids, Nucleic Acids, Sucrose, Tetracene, Lysozyme Procedure: Diacetylenes Chapter 5.3: Molecular Films and Assemblies 287 Module 5.3.1: Topography, Friction and Elasticity Measurements on Organic Thin Films 287 Module 5.3.2: Langmuir Blodgett Films 297 Procedure: AFM of Langmuir Blodgett Films 297 Module 5.3.3: STM and AFM Imaging of Alkanethiolate Monolayers at Gold Surfaces 303 Procedure: STM Imaging of Alkanethiolate Monolayers at Gold Surfaces 303 Procedure: AFM Imaging of Alkanethiolate Monolayers at Gold Surfaces 312 Procedure: STM Imaging and Etching of Alkanethiol Multilayers on Gold Surfaces 320 Module 5.3.4: DNA Bases 324 Introduction 324 Procedure: STM Imaging of DNA Bases in Air and UHV. . 325 Module 5.3.5: Aromatics 332 Procedure: STM of Phthalocyanines and Perylene Derivatives 332 Module 5.3.6: Hydrocarbons and Alcohols 340 Introduction 340 Contents xi Procedure: STM Imaging of Long Chain Alkanes 342 Procedure: STM Imaging of Long Chain Alcohols 344 Module 5.3.7: Liquid Crystals 346 Introduction 346 Procedure: STM Imaging of 8CB (n octylcyanobiphenyl) . . 347 Chapter 5.4: Molecular Mixtures Chapter 5.5: Organic Surface Treatments 352 Module 5.5.1: Silanization Part 6: Polymers (Part Editor: J. Rabe) 353 Chapter 6.1: General Considerations 355 Introduction 355 Chapter 6.2: Polymeric Materials 356 Module 6.2.1: Alkanes 356 Introduction 356 Procedure: AFM Imaging of the Lamellar Surface of n Hexatriacontane C36H74 and n Tritriacontane C33H68 Crystals 357 Procedure: AFM Imaging of the Lamellar Surfaces of Cyclic Alkanes (CH2)72, (CH2)48 358 Module 6.2.2: Semicrystalline Polymers 360 Introduction 360 Procedure: Spherulite Structure of Syndiotactic Polypropylene 361 Module 6.2.3: Epitaxially Crystallized Polymer Films 363 Introduction 363 Procedure: AFM Imaging of Epitaxially Crystallized Isotactic Polypropylene 364 Procedure: AFM Imaging of Epitaxially Crystallized Syndiotactic Polypropylene 366 Module 6.2.4: Rubbed Polymer Films 370 Procedure: Friction Transferred Polytetrafluoroethylene Thin Films 370 Module 6.2.5: Spin Coated Polymer Films 373 Introduction 373 Procedure: STM Imaging of Spin Coated Liquid Crystalline Polymer Films 375 Procedure: STM Imaging of Spin Coated Polystryene Films . 377 Module 6.2.6: Langmuir Blodgett Polymer Films Module 6.2.7: Drawn Polymer Fibres Module 6.2.8: Liquid Crystalline Polymers Module 6.2.9: Latex Film Surfaces 381 Procedure: Latex Film Surfaces Imaged by AFM 381 Module 6.2.10: Amorphous Polymers Contents xii Module 6.2.11: Block Copolymers Module 6.2.12: Polymer Blends Module 6.2.13: Conducting Polymers Chapter 6.3: Polymeric Composites Module 6.3.1: Carbon Fibre Composites Module 6.3.2: Other Composites Part 7: Biological Systems (Part Editor: A. Engel, H. Gaub) . . 385 Chapter 7.1: General Considerations 387 Chapter 7.2: DNA 389 Module 7.2.1: DNA by AFM 389 Procedure: Atomic Force Microscopy of DNA on Mica in Air and Fluid 389 Procedure: Detergent Spreading of DNA on Mica Using Nonionic and Cationic Detergents 394 Procedure: STM Imaging of DNA on a Chemically Modified Au III Surface 398 Chapter 7.3: Proteins 402 Module 7.3.1: Myosin 402 Procedure: Myosin by AFM 402 Module 7.3.2: Lysozyme 405 Procedure: Imaging Lysozyme Adsorbed on Mica by Atomic Force Microscopy 405 Module 7.3.3: Fibronectin 408 Procedure: Facile Procedure for Screening Nucleoproteins for Imagibility 408 Module 7.3.4: Cytochrome 412 Procedure: STM Analysis of Cytochrome c Immobilized on Self Assembled Monolayers on Gold 412 Module 7.3.5: Silanization (AFM) 418 Procedure: Simple Procedure for the Preparation of Positively Charged Silanated Surfaces 418 Chapter 7.4: Supported Membranes 420 Module 7.4.1: Lipid Membranes 420 Procedure: Imaging Wet Phospholipid Membranes with the AFM 420 Chapter 7.5: Protein Crystals 425 Module 7.5.1: Purple Membranes 425 Procedure: Preparation and Observation of Purple Membranes by AFM 425 Contents xiii Module 7.5.2: Porin Membranes 429 Procedure: Imaging of Reconstituted OmpF Porin in Solution using AFM 429 Module 7.5.3: HPI 433 Procedure: AFM Imaging of HPI Layers in Buffer Solution . 433 Module 7.5.4: Catalase 440 Procedure: Imaging Pt/Ir/C and W Coated Freeze Dried Catalase Crystals with STM 440 Module 7.5.5: Na+,K+ ATPase 445 Introduction 445 Procedure: Na+,K+ ATPase Imaging by AFM 446 Chapter 7.6: Filaments 452 Module 7.6.1: Microtubules 452 Procedure: Covalent Immobilization of Microtubules for AFM Studies 452 Procedure: Preparation of Microtubules for Imaging in Buffer Solution with the AFM Operated in Tapping Mode . . . 458 Module 7.6.2: Actin 460 Procedure: Preparation of Actin Filaments for Imaging in Buffer Solution with the AFM Operated in Tapping Mode 460 Module 7.6.3: Intermediate Filaments 462 Procedure: AFM Imaging of Intermediate Filaments in Buffer Solution 462 Chapter 7.7: Viruses 465 Module 7.7.1: Phage T4 Polyheads 465 Procedure: AFM Imaging of Bacteriophage T4 Polyheads in Buffer Solution 465 Chapter 7.8: Bacteria 469 Module 7.8.1: Magnetotactic Bacteria 469 Procedure: Preparation of Magnetotactic Bacteria for Force Modulation Atomic Force Microscopy 469 Chapter 7.9: Organelles 471 Module 7.9.1: Chromosomes 471 Procedure: Imaging Polytene Chromosomes 471 Module 7.9.2: Nematocysts 474 Procedure: AFM Imaging of Native Nematocysts Immobilized in Nucleopore Filters 474 Chapter 7.10: Cells 478 Module 7.10.1: Platelets 478 Procedure: Preparation of Activated Platelets for AFM Imaging 478 Module 7.10.2: Monkey Kidney Chapter 7.11: Tissues, Organisms, Plants Contents *iv Module 7.11.1: Plant Cells Chapter 7.12: Immobilization Techniques 481 Module 7.12.1: General Method 481 Procedure: A General Method for Immobilizing Biomolecules on Gold for SPM in Aqueous Buffers ... 481 Module 7.12.2: Chemical Fixation 488 Procedure: Light dependent Substrate Functionalization and Biomacromolecule Immobilization 488 Module 7.12.3: Functionalized AP mica 493 Procedure: DNA, RNA and Nucleoprotein Complexes Immobilized on AP mica and Imaged with AFM .... 493 Module 7.12.4: Tip Functionalization 497 Procedure: Functionalization of AFM Tips with Avidin. . . 497 Chapter 7.13: Intermolecular Forces 500 Module 7.13.1: DNA 500 Procedure: Quantitative Measurements of Molecular Recognition Interaction Forces with the Scanning Force Microscope 500 Part 8: Nanomanipulation Nanotechnology (Part Editor: R. Colton) 507 Introduction 507 Chapter 8.1: Manipulation of Individual Atoms Chapter 8.2: Manipulation of Individual Molecules Chapter 8.3: Manipulation of Layered Materials Chapter 8.4: Manipulation of Thin Films Chapter 8.5: Manipulation of Charged Species Chapter 8.6: Manipulation of Magnetic Species Chapter 8.7: Nanolithography and Nanofabrication 511 Module 8.7.1: STM Low Voltage E Beam Lithography 511 Introduction 511 Procedure: STM Lithography in Resists 516 Procedure: STM Nanolithography with Microposit SAL 601™ Resist 519 Procedure: Nanofabrication of GaAs with STM Lithography and Microposit SAL 601™ 524 Contents xv Procedure: Nanofabrication with STM Lithography and Self Assembling Organosilane Films 529 Module 8.7.2: Patterning on Passivated Semiconductor Surfaces. . . 535 Introduction 535 Procedure: Silicon Patterning via STM (NIST Procedure) . . 538 Procedure: Silicon Patterning via STM/AFM (NRL Procedure) 541 Procedure: Gallium Arsenide Patterning via STM 544 Module 8.7.3: STM Direct Writing of Nanostructures 546 Introduction 546 Procedure: Chemical Vapour Deposition with the STM . . . 548 Module 8.7.4: Surface Modification 553 Introduction 553 Procedure: Mechanical Surface Modification 555 Procedure: Thermal Surface Modification 558 Chapter 8.8: Application of SPM Technology Module 8.8.1: Nanoelectronics Module 8.8.2: Sensors Part 9: Materials Science on the Nanoscale (Part Editor: R. Colton) 561 Introduction 561 Chapter 9.1: Tip Surface Interactions 565 Module 9.1.1: Surface Forces Module 9.1.2: Measuring Tip Surface Interactions 565 Introduction 565 Procedure: Measuring Tip Surface Interactions using Displacement Control 568 Procedure: Measuring Tip Surface Interactions using Force Control 575 Procedure: Materials Properties Measurements 582 Module 9.1.3: Theory and Simulation Chapter 9.2: Adhesion Chapter 9.3: Nanomechanics 585 Module 9.3.1: Nanoindentation 585 Introduction 585 Procedure: Selection of Cantilevers and Tips for Nanoindentation 587 Procedure: Obtaining Raw Force Versus Separation Curve Data 592 Procedure: Derivation of Quantitative Mechanical Properties 596 Module 9.3.2: Theory and Simulation Module 9.3.3: Friction Measurements Contents xvi Chapter 9.4: Nanotribology Chapter 9.5: Nanometrology 599 Module 9.5.1: Displacement Measurements Module 9.5.2: Tip Shape Measurement/Calibration Module 9.5.3: Pitch Measurements 599 Introduction 599 Procedure: SPM Pitch Measurement of a Diffraction Grating 601 Module 9.5.4: Line Profile Measurements 603 Introduction 603 Procedure: SPM Profile Measurement of a Photoresist Line . 605 Module 9.5.5: Surface Roughness Measurements 607 Introduction 607 Procedure: Procedure Obtaining Images for Surface Roughness Measurements 608 Subject Index 619 Author Index 625
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spelling	Procedures in scanning probe microscopies ed.: Richard J. Colton ... Chichester [u.a.] Wiley 1998 XXXI, 639 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Scanning probe microscopy Rastersondenmikroskopie (DE-588)4330328-6 gnd rswk-swf Rastersondenmikroskopie (DE-588)4330328-6 s DE-604 Colton, Richard J. edt HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008075853&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis
spellingShingle	Procedures in scanning probe microscopies Scanning probe microscopy Rastersondenmikroskopie (DE-588)4330328-6 gnd
subject_GND	(DE-588)4330328-6
title	Procedures in scanning probe microscopies
title_auth	Procedures in scanning probe microscopies
title_exact_search	Procedures in scanning probe microscopies
title_full	Procedures in scanning probe microscopies ed.: Richard J. Colton ...
title_fullStr	Procedures in scanning probe microscopies ed.: Richard J. Colton ...
title_full_unstemmed	Procedures in scanning probe microscopies ed.: Richard J. Colton ...
title_short	Procedures in scanning probe microscopies
title_sort	procedures in scanning probe microscopies
topic	Scanning probe microscopy Rastersondenmikroskopie (DE-588)4330328-6 gnd
topic_facet	Scanning probe microscopy Rastersondenmikroskopie
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