A practical guide to graphite furnace atomic absorption spectrometry:
Gespeichert in:
| 1. Verfasser: | |
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| Format: | Buch |
| Sprache: | Undetermined |
| Veröffentlicht: |
New York <<[u.a.]>>
Wiley
1998
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| Schriftenreihe: | Chemical analysis
149 |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVIII, 250 S. graph. Darst. |
| ISBN: | 0471125539 |
Internformat
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Datensatz im Suchindex
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| adam_text | A PRACTICAL GUIDE TO GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY
DAVID J. BUTCHER WESTERN CAROLINA UNIVERSITY CULLOWHEE, NC JOSEPH
SNEDDON MCNEESE STATE UNIVERSITY LAKE CHARLES, LA A WILEY-INTERSCIENCE
PUBLICATION JOHN WILEY & SONS, INC. NEW YORK / CHICHESTER / WEINHEIM /
BRISBANE / SINGAPORE / TORONTO CONTENTS PREFACE ACKNOWLEDGMENTS
CUMULATIVE LISTING OF VOLUMES IN SERIES IX XI XIII CHAPTER 1
INTRODUCTION CHAPTER2 THEORY 2.1 2.2 2.3 2.4 2.5 2.6 2.7 2.8 2.9 3
SPECTROSCOPY 3 INTRODUCTION TO ATOMIC SPECTROSCOPY 4 QUANTITATIVE
CONSIDERATIONS OF TRANSITIONS 6 2.3.1 POPULATION OF ATOMS IN A STATE:
THE BOLTZMANN DISTRIBUTION 6 2.3.2 EINSTEIN COEFFICIENTS 7 ELECTRONIC
STATES OF ATOMS 8 2.4.1 QUANTUM NUMBERS FOR ELECTRONS 9 2.4.2 COUPLING
SCHEMES, TERM SYMBOLS, AND SELECTION RULES 10 2.4.3 ATOMIC SPECTRA 11
MEASURES OF TRANSITION STRENGTHS: TRANSITION PROBABILITIES AND
OSCILLATOR STRENGTHS 12 SPECTRAL PROFILES OF ABSORPTION LINES 13 GFAAS
ANALYTICAL SIGNAL: ABSORBANCE 15 INTENSITY OF ABSORBANCE IN TERMS OF
FUNDAMENTAL PARAMETERS 17 NATURE OF THE TRANSIENT GFAAS SIGNAL:
MECHANISM OF ATOM FORMATION IN A GRAPHITE FURNACE 19 2.9.1 SURFACE
PROCESSES 20 2.9.2 HETEROGENEOUS SOLID-GAS INTERACTIONS 21 2.9.3
GAS-PHASE CHEMISTRY 23 VI CONTENTS 2.9.4 PROCESSES BY WHICH ANALYTE IS
LOST FROM THE TUBE 24 2.9.5 MONTE CARLO SIMULATIONS OF ATOMIZATION
PROCESSES 25 REFERENCES 26 CHAPTER 3 QUANTITATIVE GFAAS: CALIBRATION 3.1
GENERAL ANALYTICAL METHODOLOGY 3.2 CALIBRATION GRAPHS 3.3 METHOD OF
STANDARD ADDITIONS 3.4 METHOD OF INTERNAL STANDARDIZATION 3.5 ABSOLUTE
ANALYSIS REFERENCES 31 31 32 35 36 37 38 CHAPTER 4 INSTRUMENTATION 4.1
4.2 4.3 4.4 4.5 4.6 39 LIGHT SOURCES 39 4.1.1 HOLLOW CATHODE LAMPS 40
4.1.2 ELECTRODELESS DISCHARGE LAMPS 43 4.1.3 XENON ARE LAMPS 43 4.1.4
SEMICONDUCTOR DIODE LASERS 44 GRAPHITE FURNACE 45 4.2.1 GRAPHITE TUBE
MATERIAL AND DESIGN 46 4.2.2 FURNACE HEATING CYCLE 49 4.2.3 METHODS OF
ATOMIZATION 54 WAVELENGTH SELECTORS 57 4.3.1 MONOCHROMATORS 59 4.3.2
ECHELLE MONOCHROMATORS 60 DETECTORS 60 SIGNAL PROCESSING, READOUT, AND
INSTRUMENT CONTROL 62 BACKGROUND CORRECTION 64 4.6.1 NEARBY LINE
(TWO-LINE) METHOD 64 4.6.2 CONTINUUM SOURCE METHOD 66 4.6.3
SELF-REVERSAL (SMITH-HIEFTJE) METHOD 69 4.6.4 ZEEMAN EFFECT METHOD 73
4.6.4.1 INVERSE LONGITUDINAL AC ZEEMAN 11 CONTENTS VLL 4.6.4.2 INVERSE
TRANSVERSE AC ZEEMAN 83 4.6.4.3 INVERSE TRANSVERSE DE ZEEMAN 84 4.6.5
COMPARISON OF BACKGROUND CORRECTION SYSTEMS 84 4.7 GRAPHITE FURNACE
ATOMIC EMISSION SPECTROMETRY 90 4.8 SPECTROMETER DESIGNS 92 4.8.1
SINGLE-ELEMENT INSTRUMENTS 93 4.8.2 MULTIELEMENT INSTRUMENTS 94
REFERENCES 99 CHAPTER 5 INTERFERENCE-FREE ANALYSIS 5.1 5.2 5.3 SPECTRAL
INTERFERENCES 5.1.1 SPECTRAL OVERLAPS 5.1.2 BACKGROUND ATTENUATION
CHEMICAL INTERFERENCES PHYSICAL INTERFERENCES REFERENCES 105 105 105 107
113 116 117 CHAPTER 6 SAMPLE PREPARATION AND INTRODUCTION 119 6.1 6.2
6.3 6.4 LIQUIDS GASES SOLIDS 6.3.1 6.3.2 6.3.3 6.3.4 6.3.5 6.3.6 6.3.7
6.5 WET DECOMPOSITION COMBUSTION FUSION SUMMARY OF DIGESTION PROCEDURES
SOLIDS ANALYSIS WITH SLURRY SAMPLING DIRECT SOLID SAMPLING LASER
ABLATION PRECONCENTRATION/SEPARATION METHODS 6.4.1 EXTRACTION 6.4.2
CHROMATOGRAPHY 6.4.3 FLOW INJECTION ANALYSIS 6.4.4 OTHER
PRECONCENTRATION/SEPARATION METHODS METAL SPECIATION REFERENCES 119 122
125 125 133 133 134 134 139 142 143 144 146 149 159 161 166 VLLL
CONTENTS CHAPTER 7 CHAPTER 8 CHAPTER 9 APPENDIX A APPENDIX B PRACTICAL
HINTS ON THE DETERMINATION OF ELEMENTS BY GFAAS 7. 1 APPLICABILITY 7.2
SAMPLING, SAMPLE STORAGE, AND SAMPLE PREPARATION 7.3 QUALITY CONTROL
PROCEDURES 7.4 DEVELOPMENT OF GFAAS METHODS 7.5 TROUBLESHOOTING
REFERENCES COMMERCIAL GFAAS INSTRUMENTATION: TYPES, COSTS, AND TRAINING
8.1 TYPES AND COSTS OF GFAAS INSTRUMENTATION 8.2 CONSUMABLES 8.3 SERVICE
AND MAINTENANCE 8.4 TRAINING FUTURE OF GFAAS HISTORICAL BACKGROUND A.L
EARLY WORK IN ATOMIC SPECTROSCOPY (BEFORE 1955) A.2 FLAME ATOMIC
ABSORPTION SPECTROMETRY A.3 GRAPHITE FURNACE ATOMIC ABSORPTION
SPECTROMETRY REFERENCES GFAAS LITERATURE B.L BOOKS B.2 PERIODICALS B.3
REVIEWS B.4 INTERNET RESOURCES B.5 APPLICATIONS OF GFAAS REFERENCES 175
175 176 183 185 188 195 197 197 200 200 201 203 205 205 205 205 207 209
209 210 210 211 211 212 APPENDIX C CONDITIONS FOR GFAAS 215 APPENDIX D
GLOSSARY 227 INDEX 241
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| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
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| spelling | Butcher, David J. Verfasser aut A practical guide to graphite furnace atomic absorption spectrometry David J. Butcher ; Joseph Sneddon New York <<[u.a.]>> Wiley 1998 XVIII, 250 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chemical analysis 149 Sneddon, Joseph Sonstige oth Chemical analysis 149 (DE-604)BV000008780 149 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018334464&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Butcher, David J. A practical guide to graphite furnace atomic absorption spectrometry Chemical analysis |
| title | A practical guide to graphite furnace atomic absorption spectrometry |
| title_auth | A practical guide to graphite furnace atomic absorption spectrometry |
| title_exact_search | A practical guide to graphite furnace atomic absorption spectrometry |
| title_full | A practical guide to graphite furnace atomic absorption spectrometry David J. Butcher ; Joseph Sneddon |
| title_fullStr | A practical guide to graphite furnace atomic absorption spectrometry David J. Butcher ; Joseph Sneddon |
| title_full_unstemmed | A practical guide to graphite furnace atomic absorption spectrometry David J. Butcher ; Joseph Sneddon |
| title_short | A practical guide to graphite furnace atomic absorption spectrometry |
| title_sort | a practical guide to graphite furnace atomic absorption spectrometry |
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