Development of a passive sampling device for combined chemical and toxicological long-term monitoring of groundwater:
Gespeichert in:
| 1. Verfasser: | |
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| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Leipzig
UFZ
2004
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| Schriftenreihe: | Umweltforschungszentrum <Leipzig>: UFZ-Bericht
2004,23 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Zsfassung in dt. Sprache |
| Beschreibung: | XII, 91, XI S. Ill., graph. Darst. |
Internformat
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Datensatz im Suchindex
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| adam_text | IMAGE 1
TABLE OF CONTENTS
TABLE OF CONTENTS
SUMMARY . ...?. ./...../. IX
ZUSAMMENFASSUNG
CHAPTER 1: GENERAL INTRODUCTION 1
1.1 CURRENT SAMPLING STRATEGIES 1
1.2 APPROACHES FOR COMBINED CHEMICAL AND BIOLOGICAL MONITORING 2
1.3 AIM AND STRUCTURE OF THIS MESIS 4
CHAPTER 2: AQUEOUS PHASE PASSIVE SAMPLING - AN OVERVIEW 5
2.1 INTRODUCTION 5
2.2 PRINCIPLES UNDERLYING PASSIVE SAMPLERS 6
2.2.1 ASSEMBLY 6
2.2.2 EQUILIBRIUM VS. NON-EQUILIBRIUM SAMPLERS 7
2.3 OVERVIEW OF PASSIVE SAMPLERS SUITABLE FOR GROUND- AND SURFACE WATER
8
2.4 CHEMICAL ANALYSIS AND EVALUATION OF PASSIVELY COLLECTED CONTAMINANTS
11
2.5 FACTORS TO BE CONSIDERED IN THE APPLICATION OF PASSIVE SAMPLING
DEVICES 13
2.6 CURRENT TRENDS IN PASSIVE WATER SAMPLING 15
2.7 CONCLUSIONS WITH REGARD TO THIS THESIS 16
CHAPTER 3: DEVELOPMENT OF A SOLVENT-FREE, SOLID-PHASE BIOASSAY 17
3.1 INTRODUCTION 17
3.2 MATERIALS AND METHODS 21
3.2.1 CHEMICALS AND SORBENTS 21
3.2.2 HPLC ANALYSIS OF PAH SOLUTIONS AND SORBENT EXTRACTS 22
3.2.3 CEIL CULTIVATION AND PERFORMANCE OFBIOASSAYS 23
3.2.4 EROD AND CELL VIABILITY ASSAYS 24
3.2.5 COATING OF SORBENT BEADS 25
3.2.6 COMPATIBILITY OF SORTXNT MATERIALS WITH FISH CEIL LINES 25
3.2.7 EXPOSURE OF CELLS WITH PAH-COATEDSORBENTMATERIALS (BEAD ASSAY) 25
3.2.8 EXPOSURE TO PAHSIN THE STANDARD ASSAY 26
3.2.9 DISTRIBUTION OFPAHS WITHIN BEAD AND STANDARD EROD ASSAY 27
3.3 RESULTS 28
3.3.1 COMPATIBILITY OF SORBENT MATERIALS WITH FISH CELL CULTURES AND
FLUORESCENT DYE BIOASSAYS 28
3.3.2 EROD INDUCTION ELICITED BY PAH CONTAMINATED SORBENT BEADS 30
3.3.3 ROLE OF SORPTION IN THE EROD RESPONSE 31
3.3.4 DISTRIBUTION OF PAHS IN BEAD AND STANDARD EROD-ASSAY 32
3.3.5 COMPARISON OF STANDARD AND BEAD ASSAY 34
3.4 DISCUSSION 36
3.5 SUMMARY 38
III
IMAGE 2
TABLE OF CONTENTS
CHAPTER 4: TOXIMETER DEVELOPMENT: EVALUATING THE APPLICABILITY OF THE
BIOSILON FILLED CERAMIC TUBE PASSIVE SAMPLER IN LABORATORY EXPERIMENTS
39
4.1 INTRODUCTION 39
4.1.1 TOXIMETER DESIGN 40
4.2 MATERIALS AND METHODS 42
4.2.1 CHEMICALS ANDSORBENTS 42
4.2.2 INSTRUMENTAL ANALYSIS 42
4.2.3 OPTIMIZATION OF THE EXTRACTION PROTOCOL FOR BIOSILON 43
4.2.4 ASSESSMENT OF THE PARTITIONING OF PAHS BETWEEN WATER AND BIOSI/ON
43
4.2.5 TOXIMETER PREPARATION 44
4.2.6 PROCESSING OF THE TOXIMETER AFTER SAMPLING 45
4.2.7 PROCESSING OF WATER SAMPLES 45
4.2.8 PERFONNANCE OF BIOASSAYS 46
4.2.9 LABORATORY EXPOSURE SCENARIOS FOR CALIBRATION OF THE TOXIMETER 46
4.3 RESULTS 48
4.3.1 OPTIMIZATION OF THE EXTRACTION PROTOCOL FOR BIOSIION 48
4.3.2 ASSESSMENT OF THE PARTITIONING OF PAHS BETWEEN WATER AND BIOSILON
49
4.3.3 LABORATORY EXPOSURE SCENARIOS FOR CALIBRATION OF THE TOXIMETER 52
4.4 DISCUSSION 61
4.4.1 BIOSILON AS A RECEIVING PHASE FOR PAHS 61
4.4.2 LABORATORY EXPOSURE SCENARIOS FOR CALIBRATION OF THE TOXIMETER 62
4.5 SUMMARY 64
CHAPTER 5: TOXIMETER FIELD DEPLOYMENT 65
5.1 INTRODUCTION 65
5.2 MATERIALS AND METHODS 66
5.2.1 SAMPLING SITE 66
5.2.2 PASSIVE SAMPLER PREPARATION 66
5.2.3 PASSIVE SAMPLER FIELD DEPLOYMENT 67
5.2.4 SAMPLING 67
5.2.5 PROCESSINGOFPASSIVESAMPLERAFTERFIELD DEPLOYMENT 68
5.2.6 INSTRUMENTAL ANALYSIS 68
5.3 RESULTS 69
5.3.1 VISIBLE CHANGES OF PASSIVE SAMPLERS A FLIER FIELD EXPOSURE 69
5.3.2 TOXIMETER SAMPLES 69
5.3.2 CERAMIC DOSIMETER SAMPLES 76
5.4 DISCUSSION 78
5.5 SUMMARY 80
CHAPTER 6: CONCLUDING REMARKS AND FUTURE DIRECTIONS 81
REFERENCES 84
APPENDIX I
IV
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| language | English |
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| spelling | Bopp, Stephanie 1975- Verfasser (DE-588)129643637 aut Development of a passive sampling device for combined chemical and toxicological long-term monitoring of groundwater vorgelegt von Stephanie Bopp Leipzig UFZ 2004 XII, 91, XI S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Umweltforschungszentrum <Leipzig>: UFZ-Bericht 2004,23 Zsfassung in dt. Sprache Zugl.: Rostock, Univ., Diss., 2004 Grundwasserüberwachung (DE-588)4325734-3 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Grundwasserüberwachung (DE-588)4325734-3 s DE-604 Umweltforschungszentrum <Leipzig>: UFZ-Bericht 2004,23 (DE-604)BV010126205 2004,23 SWB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=013028843&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Bopp, Stephanie 1975- Development of a passive sampling device for combined chemical and toxicological long-term monitoring of groundwater Umweltforschungszentrum <Leipzig>: UFZ-Bericht Grundwasserüberwachung (DE-588)4325734-3 gnd |
| subject_GND | (DE-588)4325734-3 (DE-588)4113937-9 |
| title | Development of a passive sampling device for combined chemical and toxicological long-term monitoring of groundwater |
| title_auth | Development of a passive sampling device for combined chemical and toxicological long-term monitoring of groundwater |
| title_exact_search | Development of a passive sampling device for combined chemical and toxicological long-term monitoring of groundwater |
| title_full | Development of a passive sampling device for combined chemical and toxicological long-term monitoring of groundwater vorgelegt von Stephanie Bopp |
| title_fullStr | Development of a passive sampling device for combined chemical and toxicological long-term monitoring of groundwater vorgelegt von Stephanie Bopp |
| title_full_unstemmed | Development of a passive sampling device for combined chemical and toxicological long-term monitoring of groundwater vorgelegt von Stephanie Bopp |
| title_short | Development of a passive sampling device for combined chemical and toxicological long-term monitoring of groundwater |
| title_sort | development of a passive sampling device for combined chemical and toxicological long term monitoring of groundwater |
| topic | Grundwasserüberwachung (DE-588)4325734-3 gnd |
| topic_facet | Grundwasserüberwachung Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=013028843&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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