Physical and chemical methods of separation:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
New York [u.a.]
McGraw-Hill
1963
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIV, 366 S. Ill., graph. Darst. |
Internformat
MARC
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| 100 | 1 | |a Berg, Eugene W. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Physical and chemical methods of separation |c Eugene W. Berg |
| 264 | 1 | |a New York [u.a.] |b McGraw-Hill |c 1963 | |
| 300 | |a XIV, 366 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 4 | |a Cromatografía | |
| 650 | 4 | |a Intercambio de iones | |
| 650 | 4 | |a Iones | |
| 650 | 4 | |a Separación (Tecnología) | |
| 650 | 0 | 7 | |a Chemisches Labor |0 (DE-588)4009880-1 |2 gnd |9 rswk-swf |
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Datensatz im Suchindex
| _version_ | 1804116574133551104 |
|---|---|
| adam_text | Contents
Preface, vii
Chapter 1. Introduction, 1
1.1. The Scope and Aims of Separation Methods, 1
1.2. Classification of Separation Methods, 2
1.3. Distillation, 5
1.4. Solvent Extraction, 6
1.5. Chromatography, 7
1.6. Ring-oven Technique, 8
1.7. Zone Melting, 8
1.8. Ion Exchange, 8
1.9. Ion Exclusion, 10
1.10. Dialysis, 11
1.11. Precipitation, Coprecipitation, and Adsorption, 12
1.12. Flotation, 13
1.13. Biological Methods, 14
Chapter 2. Fractional Distillation and Sublimation, 15
2.1. Basic Principles of Distillation, 15
2.2. Theory of Fractional Distillation, 18
2.3. Analysis of the Steady-state Condition (Continuous Distillation),
21
2.4. Analysis of Batch Fractional Distillation, 26
2.5. Apparatus, 28
2.6. General Applications, 32
2.7. Fractional Distillation of Organics, 33
2.8. Fractional Distillation of Inorganics, 36
2.9. Molecular Distillation, 39
2.10. Sublimation, 42
2.11. Selected Bibliography, 47
Chapter 3. Liquid-Liquid Extraction, 50
3.1. Distribution Law, 50
x CONTENTS
3.2. Deviations from the Distribution law, 52
3.3. Triangular Coordinates, 53
3.4. Choice of Solvent, 54
3.5. Techniques of Extraction, 58
3.6. Batch Extractions, 60
3.7. Multiple Extractions, 63
3.8. Countercurrent Extraction, 66
3.9. Extraction of Solids, 73
3.10. Advantages, 73
3.11. Disadvantages, 73
3.12. Applications, 74
3.13. Selected Bibliography, 78
Chapter 4- Adsorption Chromatography, 80
4.1. History, 80
4.2. Development of Chromatogram, 81
4.3. Frontal Analysis, 84
4.4. Displacement Analysis, 85
4.5. EHution Analysis, 86
4.6. Gradient Elution Analysis, 87
4.7. Present Status of Theory, 88
4.8. Adsorbents, 91
4.9. Adsorption Sequence of Functional Groups, 95
4.10. Solvents, 96
4.11. Apparatus, 96
4.12. Detection of Zones, 98
4.13. Applications, 100
4.14. Advantages and Disadvantages, 103
4.15. Partition Chromatography, 103
4.16. Selected Bibliography, 105
Chapter 5. Gas Chromatography, 107
5.1. Introduction, 107
5.2. Theory, 108
5.3. Elfficiency of a Column, 111
5.4. Mobile Phase, 114
5.5. Presentation of Data, 116
5.6. Instrumentation, 117
5.7. Applications, 126
5.8. Limitations, 130
5.9. Selected Bibliography, 130
CONTENTS xi
Chapter 6. Paper Chromatography, 133
6.1. Introduction, 133
6.2. Physical and Chemical Properties of Cellulose, 134
6.3. Adsorption Mechanisms Involving Cellulose, 13.5
6.4. Apparatus, 136
6.5. One-dimensional Chromatography, 137
6.6. Two-dimensional Chromatography, 138
6.7. Detection of Zones, 139
6.8. Applications, 140
6.9. Advantages and Disadvantages, 141
6.10. Selected Bibliography, 141
Chapter 7. Electrochromatography (Zone Electrophoresis), 143
7.1. Introduction, 143
7.2. Theory, 146
7.3. Apparatus, 147
7.4. Applications, 150
7.5. Selected Bibliography, 153
Chapter 8. The Ring-oven Technique, 155
8.1. Introduction, 155
8.2. Apparatus, 156
8.3. Separations for Qualitative Analysis, 158
8.4. Selected Bibliography, 162
Chapter 9. Zone Melting, 163
9.1. Introduction, 163
9.2. Theory, 165
9.3. Apparatus, 170
9.4. Applications, 172
9.5. Selected Bibliography, 175
Chapter 10. Ion Exchange. 176
10.1. Introduction, 176
10.2. Ion-exchange Resins (Structure), 178
10.3. Ion-exchange Equilibria, 183
10.4. Ion-exchange Kinetics, 191
10.5. Techniques of Ion Exchange, 193
10.6. Apparatus, 202
10.7. Deionization of Aqueous Solutions, 204
xii CONTENTS
10.8. Water Softening, 206
10.9. Concentration of Electrolytes, 207
10.10. Preparation of Reagents, 207
10.11. Dissolution of Insoluble Electrolytes, 208
10.12. Removal of Interfering Ions, 209
10.13. Ion-exchange Chromatography, 209
10.14. Selected Bibliography, 214
Chapter 11. Ion Exclusion, 217
11.1. Introduction, 217
11.2. Distribution Phenomenon, 217
11.3. Theory, 220
11.4. Applications, 222
11.5. Advantages and Disadvantages 224
11.6. Ion Retardation, 225
11.7. Selected Bibliography, 226
Chapter 12. Dialysis, 227
12.1. Introduction, 227
12.2. Theory, 229
12.3. Membranes, 232
12.4. Apparatus, 237
12.5. Applications, 238
12.6. Selected Bibliography, 240
Chapter 13. Electrodialysis and Ion-exchange Membranes, 242
13.1. Introduction, 242
13.2. Principles of Membrane Selectivity to Anions or Cations, 243
13.3. Ion-exchange Membranes, 244
13.4. Apparatus, 245
13.5. General Applications, 245
13.6. Desalinization of Brackish Water, 247
13.7. Selected Bibliography, 249
Chapter 14. Precipitation, 250
14.1. Introduction, 250
14.2. The Effect of Temperature on Solute Solubility, 251
14.3. The Effect of Pressure on Solute Solubility, 254
14.4. The Effect of Particle Size on Solute Solubility, 256
14.5. The Effect of Supersaturation on Solute Solubility, 259
14.6. The Effect of Solvent on Solute Solubility, 263
CONTENTS xiii
14.7. The Effect of Salt Concentration on Solute Solubility, 2(57
14.8. The Effect of Complex Ion Formation on Solute Solubility, 273
14.9. The Effect of pH on Solute Solubility, 276
14.10. Precipitation from a Homogeneous Alodium, 279
14.11. Fractional Precipitation, 285
14.12. Precipitate Exchange Reactions, 28(3
14.13. Organic Precipitants, 288
14.14. Selected Bibliography, 293
Chapter 15. Coprecipitation, Adsorption,
and Postprecipitation, 296
15.1. Coprecipitation, 296
15.2. Mechanism and Extent of Adsorption, 297
15.3. Separations Achieved with Coprecipitation Processes, 302
15.4. Postprecipitation, 306
15.5. Selected Bibliography, 309
Chapter 16. Flotation, S10
16.1. Introduction, 310
16.2. Topochemical Reactions, 310
16.3. General Properties of the Solid State, 311
16.4. Heterogeneity of Solid Surfaces, 312
16.5. Partial Mobility of Solid Surfaces, 314
16.6. Adhesion between Solids and Liquids, 314
16.7. Measurement of Contact Angles, 317
16.8. Stabilization of a Solid in a Gas-Liquid Interface, 319
16.9. Flotation, 323
16.10. Collectors, 325
16.11. Mechanism by Which Collectors Function, 327
16.12. Modulation of Collector Action, 330
16.13. Applications, 331
16.14. Selected Bibliography, 333
Chapter 17. Biological Methods, 335
17.1. Introduction, 335
17.2. Metabolic Selectivity of Plants, 337
17.3. Metabolic Selectivity of Animals, 338
17.4. Metabolic Selectivity of Microorganisms, 338
17.5. Suggested Exploitation of Living Cells for Isolating and Concen-
trating Substances, 340
17.6. Selected Bibliography, 341
xiv CONTENTS
Chapter 18. Elimination of Undesired Reactions through Use
of Sequestering (Masking) Agents, 343
18.1. Introduction, 343
18.2. Methods and Scope, 344
18.3. Masking of Individual Ions, 347
18.4. Demasking, 354
18.5. Selected Bibliography, 356
Index, 359
|
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| indexdate | 2024-07-09T15:40:40Z |
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| language | English |
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| physical | XIV, 366 S. Ill., graph. Darst. |
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| spelling | Berg, Eugene W. Verfasser aut Physical and chemical methods of separation Eugene W. Berg New York [u.a.] McGraw-Hill 1963 XIV, 366 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Cromatografía Intercambio de iones Iones Separación (Tecnología) Chemisches Labor (DE-588)4009880-1 gnd rswk-swf Trennverfahren (DE-588)4078395-9 gnd rswk-swf Chemisches Labor (DE-588)4009880-1 s Trennverfahren (DE-588)4078395-9 s DE-604 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001390607&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Berg, Eugene W. Physical and chemical methods of separation Cromatografía Intercambio de iones Iones Separación (Tecnología) Chemisches Labor (DE-588)4009880-1 gnd Trennverfahren (DE-588)4078395-9 gnd |
| subject_GND | (DE-588)4009880-1 (DE-588)4078395-9 |
| title | Physical and chemical methods of separation |
| title_auth | Physical and chemical methods of separation |
| title_exact_search | Physical and chemical methods of separation |
| title_full | Physical and chemical methods of separation Eugene W. Berg |
| title_fullStr | Physical and chemical methods of separation Eugene W. Berg |
| title_full_unstemmed | Physical and chemical methods of separation Eugene W. Berg |
| title_short | Physical and chemical methods of separation |
| title_sort | physical and chemical methods of separation |
| topic | Cromatografía Intercambio de iones Iones Separación (Tecnología) Chemisches Labor (DE-588)4009880-1 gnd Trennverfahren (DE-588)4078395-9 gnd |
| topic_facet | Cromatografía Intercambio de iones Iones Separación (Tecnología) Chemisches Labor Trennverfahren |
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