Morphology and growth of titania nanotubes: nanostructuring and applications = (Morphologie und Wachstum von Titandioxid-Nanoröhren)
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
2012
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| Schlagworte: | |
| Online-Zugang: | kostenfrei http://d-nb.info/1028852185/34 https://nbn-resolving.org/urn:nbn:de:bvb:29-opus-37311 Inhaltsverzeichnis |
| Beschreibung: | III, 183 S. Ill., graph. Darst. |
Internformat
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| 245 | 1 | 0 | |a Morphology and growth of titania nanotubes |b nanostructuring and applications = (Morphologie und Wachstum von Titandioxid-Nanoröhren) |c von Sergiu P. Albu |
| 246 | 1 | 1 | |a (Morphologie und Wachstum von Titandioxid-Nanoröhren) |
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Datensatz im Suchindex
| _version_ | 1804149982026006528 |
|---|---|
| adam_text | IMAGE 1
CONTENTS
CONTENTS
ABSTRACT 1
1 OVERVIEW 5
1.1 INTRODUCTION 5
1.2 PROPERTIES OF TITANIUM DIOXIDE 6
1.3 THE AIM OF THIS WORK 7
2 THEORETICAL ISSUES 9
2.1 PASSIVATION OF METALS. COMPACT ANODIC OXIDES 9
2.2 DISSOLUTION AND POROSIFICATION OF METAL OXIDES 17
3 EXPERIMENTAL AND ANALYTICAL INSTRUMENTS 29
3.1 ELECTROCHEMICAL SET-UP 29
3.2 ELECTRON MICROSCOPY TECHNIQUES 32
3.3 X-RAY DIFFRACTION ANALYSIS 35
3.4 HEAT TREATMENT SET-UPS 3 8
4 EXPERIMENTAL METHODOLOGY 39
4.1 AN OVERVIEW O F TITANIUM SAMPLES 39
4.2 IMPORTANCE OF PRE- AND POST-TREATMENTS 39
4.3 IMPACT O F T H E ELECTROCHEMICAL CELL DESIGN ON ANODIZATION 4 1
5 FORMATION AND GROWTH OF TIO Z NANOTUBES 45
5.1 GENERAL ASPECTS OF GROWTH OF TI0 2 NANOTUBULAR ARRAYS 45
5.2 GROWTH SEQUENCE 4 7
5.3 DETAILED GEOMETRIC ASPECTS OF THE NANOTUBES 5 0
5.4 CHEMICAL COMPOSITION O F T H E NANOTUBES 5 7
5.5 INFLUENCE OF T H E FLUORIDE CONCENTRATION 60
5.6 EFFECT OF ANODIZATION VOLTAGE 6 3
5.7 INFLUENCE OF T H E WATER CONTENT IN T H E ELECTROLYTE 65
5.8 EFFECT OF T H E ELECTROLYTE PH 69
5.9 INFLUENCE OF TEMPERATURE 7 2
5.10 IMPACT O F T H E BACKGROUND ELECTROLYTE 75
5.11 EFFICIENCIES OF NANOTUBE FORMATION AND GROWTH 8 0
5.12 OTHER ASPECTS OF T1O2 NANOTUBE GROWTH 9 0
I I P A G E
HTTP://D-NB.INFO/1030501084
IMAGE 2
CONTENTS
6 CRYSTALLIZATION OF TI0 2 NANOTUBES 97
6.1 THERMAL CRYSTALLIZATION OF TI0 2 N A N O T U B E S 9 7
6.1.1 AN OVERVIEW OF TI0 2 CRYSTALLIZATION AND PHASE TRANSITIONS 9 7
6.1.2 TEMPERATURE IMPACT ON T H E TI0 2 N A N O T U B E S 9 8
6.1.3 IMPORTANCE OF THERMAL RAMP DURING CRYSTALLIZATION 107
6.2 E-BEAM CRYSTALLIZATION OF TIC 2 NANOTUBES 110
7 ADVANCED NANOSTRUCTURES AND APPLICATIONS 113
7.1 HIGHLY DEFINED AND ORDERED TOP-OPENINGS OF TI0 2 N A N O T U B E S
113
7.1.1 FABRICATION TECHNIQUES 113
7.1.2 IMPACT ON DYE-SENSITIZED SOLAR CELLS 117
7.2 TI0 2 NANOTUBULAR MEMBRANES 118
7.2.1 DETACHING STRATEGIES FOR TI0 2 N A N O T U B E S 118
7.2.2 OPENING TUBE BOTTOMS TECHNIQUES 120
7.2.3 MEMBRANE HANDLING VIA PHOTOLITHOGRAPHY 124
7.2.4 APPLICATIONS 128
7.3 BAMBOO- AND BRANCHED-TYPE TI0 2 N A N O T U B E S 133
7.3.1 FORMATION MECHANISM OF BAMBOO-TYPE NANOTUBES 133
7.3.2 FORMATION OF BRANCHED TI0 2 N A N O T U B E S 136
7.4 TI0 2 NANOLACE - A CHEMICAL ETCHING PRODUCT OF BAMBOO-TYPE NANOTUBES
138
7.4.1 FORMATION OF TI0 2 NANOLACES 138
7.4.2 PROPERTIES OF NANOLACE SHEETS 139
8 CONCLUSIONS 141
9 FURTHER WORK 145
10 APPENDIXES 147
A1 HYGROSCOPY OF ETHYLENE GLYCOL 147
A2 THERMAL SENSORS 148
A3 SET-UP CONFIGURATION 150
A4 EXAMPLE O F T H E PROGRAM CODE 152
A5 IMPACT OF SURFACE STATE ON T H E INITIATION OF TI0 2 N A N O T U B E
S 155
A6 CRYSTALLIZATION OF ORDERED POROUS STRUCTURES IN WATER 157
A7 ELECTROCHEMICAL IMPEDANCE SPECTROSCOPY OF TI0 2 N A N O T U B E S 159
A8 AES AND TOF SIMS ANALYSES OF TI0 2 N A N O T U B E S 160
1 1 | P A G E
IMAGE 3
CONTENTS
A9 PROPERTIES OF SOME POLAR SOLVENTS 162
A10 GIANT NANOTUBES 166
A L L GROWING NANOTUBES ON THIN TI WIRE 167
11 BIBLIOGRAPHY 169
12 LIST OF ABBREVIATIONS AND SYMBOLS 179
13 LIST OF PUBLICATIONS 181
III | P A G E
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| discipline | Maschinenbau / Maschinenwesen |
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| spelling | Albu, Sergiu P. Verfasser aut Morphology and growth of titania nanotubes nanostructuring and applications = (Morphologie und Wachstum von Titandioxid-Nanoröhren) von Sergiu P. Albu (Morphologie und Wachstum von Titandioxid-Nanoröhren) 2012 III, 183 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Erlangen-Nürnberg, Univ., Diss., 2012 Titandioxid (DE-588)4185549-8 gnd rswk-swf Nanoröhre (DE-588)4844582-4 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Titandioxid (DE-588)4185549-8 s Nanoröhre (DE-588)4844582-4 s DE-604 Erscheint auch als Online-Ausgabe urn:nbn:de:bvb:29-opus-37311 https://open.fau.de/handle/openfau/2676 Verlag kostenfrei Volltext http://d-nb.info/1028852185/34 Langzeitarchivierung Nationalbibliothek https://nbn-resolving.org/urn:nbn:de:bvb:29-opus-37311 Resolving-System DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025667068&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Albu, Sergiu P. Morphology and growth of titania nanotubes nanostructuring and applications = (Morphologie und Wachstum von Titandioxid-Nanoröhren) Titandioxid (DE-588)4185549-8 gnd Nanoröhre (DE-588)4844582-4 gnd |
| subject_GND | (DE-588)4185549-8 (DE-588)4844582-4 (DE-588)4113937-9 |
| title | Morphology and growth of titania nanotubes nanostructuring and applications = (Morphologie und Wachstum von Titandioxid-Nanoröhren) |
| title_alt | (Morphologie und Wachstum von Titandioxid-Nanoröhren) |
| title_auth | Morphology and growth of titania nanotubes nanostructuring and applications = (Morphologie und Wachstum von Titandioxid-Nanoröhren) |
| title_exact_search | Morphology and growth of titania nanotubes nanostructuring and applications = (Morphologie und Wachstum von Titandioxid-Nanoröhren) |
| title_full | Morphology and growth of titania nanotubes nanostructuring and applications = (Morphologie und Wachstum von Titandioxid-Nanoröhren) von Sergiu P. Albu |
| title_fullStr | Morphology and growth of titania nanotubes nanostructuring and applications = (Morphologie und Wachstum von Titandioxid-Nanoröhren) von Sergiu P. Albu |
| title_full_unstemmed | Morphology and growth of titania nanotubes nanostructuring and applications = (Morphologie und Wachstum von Titandioxid-Nanoröhren) von Sergiu P. Albu |
| title_short | Morphology and growth of titania nanotubes |
| title_sort | morphology and growth of titania nanotubes nanostructuring and applications morphologie und wachstum von titandioxid nanorohren |
| title_sub | nanostructuring and applications = (Morphologie und Wachstum von Titandioxid-Nanoröhren) |
| topic | Titandioxid (DE-588)4185549-8 gnd Nanoröhre (DE-588)4844582-4 gnd |
| topic_facet | Titandioxid Nanoröhre Hochschulschrift |
| url | https://open.fau.de/handle/openfau/2676 http://d-nb.info/1028852185/34 https://nbn-resolving.org/urn:nbn:de:bvb:29-opus-37311 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025667068&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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