Materialwissenschaftliche Untersuchungen zur Oberflächenmodifizierung von Kohlenstofffasern in faserverstärkten Metallkompositen:
Gespeichert in:
| 1. Verfasser: | |
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| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Dresden
Oktober 2016
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Beschreibung: | VIII, 131 Seiten Illustrationen, Diagramme 21 cm |
Internformat
MARC
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| 245 | 1 | 0 | |a Materialwissenschaftliche Untersuchungen zur Oberflächenmodifizierung von Kohlenstofffasern in faserverstärkten Metallkompositen |c vorgelegt von Alfaferi Zainal Abidin |
| 264 | 1 | |a Dresden |c Oktober 2016 | |
| 300 | |a VIII, 131 Seiten |b Illustrationen, Diagramme |c 21 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |b Dissertation |c Technische Universität Dresden |d 2017 | ||
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Datensatz im Suchindex
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| adam_text | TABLE OF CONTENTS
ACKNOWLEDGEMENT I
ABSTRACT II
TABLE OF CONTENTS III
LIST OF ABBREVIATIONS V
LIST OF SYMBOLS VII
1. GENERAL INTRODUCTION AND OBJECTIVES OF THE DISSERTATION 1
2. CARBON FIBER REINFORCED MATAL MATRIX COMPOSITES (CF/MMCS) 3
2.1. COMPONENTS OF FIBER REINFORCED METAL MATRIX COMPOSITES (CF/MMCS)
2.1.1. ALUMINUM ALLOYS (AL-ALLOYS)
2.1.2. MAGNESIUM ALLOYS (MG-ALLOYS)
2.1.3. CARBON FIBER
2.1.3.1. PROPERTIES, STRUCTURES AND TYPES
2.1.3.2. CARBON FIBER PRODUCTION PROCESS
2.2. FABRICATION OF
CF/MMCS
BY LIQUID METAL INFILTRATION
2.2.1. GAS PRESSURE INFILTRATION (GPI)
2.2.2. DIRECT SQUEEZE CASTING 10
2.2.3. HIGH PRESSURE DIE CASTING (HPDC) 11
2.3. WETTING BETWEEN FIBERS AND METAL MATRIX 11
2.3.1. THE ROLE OF WETTING 11
2.3.2. TAILORING OF FIBER-MATRIX INTERFACE IN
CF/MMCS
12
2.4. STATE OF THE ART CARBON FIBER COATINGS FOR THE USE IN METAL
MATRIX COMPOSITES (MMCS) 14
3. DEPOSITION METHODS FOR FIBER COATING 18
3.1. SOL-GEL TECHNIQUE 18
3.2. MOLTEN SALT TECHNIQUE 18
3.3. PHYSICAL VAPOR DEPOSITION (PVD) 18
3.4. ELECTROPLATING 19
3.5. ELECTROLESS PLATING 19
3.6. CHEMICAL VAPOR DEPOSITION (CVD) 20
3.6.1. GENERAL INFORMATION 20
3.6.2. THERMODYNAMICS OF CVD 22
3.6.3. DEPOSITION MECHANISM AND MASS TRANSPORT PHENOMENA 23
3.6.4. KINETICS OF CVD 26
3.6.5. THIN FILM GROWTH 29
3.7. ATOMIC LAYER DEPOSITION (ALD) 30
3.7.1. GENERAL INFORMATION 30
3.7.2. ALD PROCESS WINDOW 31
3.7.3. ALD REACTOR TYPES AND PRECURSOR REQUIREMENTS 32
4. BASICS AND STATE OF THE ART OF TIN,
AI2O3
AND TIS
2
/TIN 34
4.1. CVD OF TITANIUM NITRIDE (TIN) 34
4.2. ALD OF ALUMINUM OXIDE
(AI2O3)
37
4.3. CVD OF TITANIUM DISULFIDE (T
1
S
2
) 40
(0(0000)0 AI-TW-^
5. EXPERIMENTAL WORK
42
5.1. COATING OF CARBON FIBERS 42
5.1.1. CVD OF TITANIUM NITRIDE (TIN) 42
5.1.2. CVD OF TITANIUM DISULFIDE (TIS2) AND DOUBLE LAYER TIS2/TIN 43
5.1.3. A L D O FA H O S 43
5.2. MATERIALS 44
5.3. COMPOSITE MANUFACTURE BY GAS PRESSURE INFILTRATION (GPI) 45
5.4. ANALYTICAL METHODS 46
5.4.1. SCANNING ELECTRON MICROSCOPY (SEM) 46
5.4.2. TRANSMISSION ELECTRON MICROSCOPY (TEM) 47
5.4.3. X-RAY PHOTOELECTRON SPECTROSCOPY (XPS) 48
5.4.4. THERMOGRAVIMETRIC ANALYSES (TGA) 49
5.4.5. X-RAY DIFFRACTION ANALYSIS (XRD) 49
5.4.6. SESSILE DROP TEST 50
5.4.7. TENSILE STRENGTH OF COATED FIBERS 51
6. RESULT AND DISCUSSION 53
6.1. THERMAL TREATMENT OF CARBON FIBERS PRIOR TO DEPOSITION 53
6.2. CVD OF TITANIUM NITRIDE (TIN) 54
6.2.1. STRUCTURE, COMPOSITION AND THICKNESS HOMOGENEITY OF TIN COATINGS
55
6.2.2. OXIDATION BEHAVIOR AND TENSILE STRENGTH OF UNCOATED AND COATED
FIBERS 59
6.2.3. WETTABILITY TEST AND INTERFACE ANALYSIS OF AI/TIN/CGR 60
6.3. ALD OF ALUMINUM OXIDE (AL203) 62
6.3.1. STRUCTURE, COMPOSITION AND THICKNESS HOMOGENEITY OF ALUMINA
COATINGS 63
6.3.2. OXIDATION BEHAVIOR AND TENSILE STRENGTH OF AI203-COATED
HM-/HT-FIBERS 66
6.3.2.1 HTS40 FIBERS (HIGH TENACITY) 66
6.3.2.2 M40J FIBERS (HIGH MODULUS) 67
6.3.3. WETTABILITY TEST OF AI203-COATED GRAPHITE WITH CP-AI AND ALSICU
(226D) 68
6.4. CVD OF TITANIUM DISULFIDE (TIS2) AND TIS2/TIN DOUBLE COATINGS 69
6.4.1. THERMODYNAMIC ANALYSIS OF THE CVD SYSTEM TI-S-CI-H-AR 69
6.4.2. STRUCTURE, COMPOSITION AND DEPOSITION RATE OF TIS2 COATING
DEPOSITED ON PLANAR
GRAPHITE SUBSTRATE 71
6.4.3. STRUCTURE AND THICKNESS HOMOGENEITY OF TIS2 SINGLE COATINGS AND
TISX/TIN
DOUBLE COATINGS ON CARBON FIBER FABRICS 80
6.4.4. OXIDATION BEHAVIOR AND TENSILE STRENGTH OF UNCOATED AND COATED
FIBERS 83
6.5. MMC BY INFILTRATION OF UNCOATED AND COATED CARBON FIBER FABRICS 85
6.5.1. INFILTRATION OF TIN-COATED 3D-HTS-TEXTILE PREFORM WITH 226D BY
GPI METHOD 85
6.5.2. INFILTRATION OF TIN-COATED 2D/3D-HTS-TEXTILE PREFORM WITH AZ91 BY
GPI METHOD 89
6.5.3. INFILTRATION OF UNCOATED- AND AI203-COATED 2D-HM-TEXTILE PREFORM
WITH
226D BY GPI METHOD 93
6.5.4. INFILTRATION OF UNCOATED- AND AI203-COATED 2D-HM-TEXTILE PREFORM
WITH
239D BY GPI METHOD 98
6.5.5. INFILTRATION OF UNCOATED- AND AI203-COATED 2D -H TS TEXTILE
PREFORM WITH
AZ91 BY GPI METHOD 101
6.5.6. INFILTRATION BEHAVIOR OF TIN-AND AI203-COATED 3D-HTS-TEXTILE
PREFORMS WITH
226D BY HPDC METHOD 105
7. SUMMARY AND OUTLOOK 106
8. DIRECTORIES 110
8.1. REFERENCES 110
8.2. LIST OF FIGURES 123
8.3. LIST OF TABLES 130
8.4. LIST OF PUBLICATIONS RELATED WITH THIS WORK 131
|
| adam_txt |
TABLE OF CONTENTS
ACKNOWLEDGEMENT I
ABSTRACT II
TABLE OF CONTENTS III
LIST OF ABBREVIATIONS V
LIST OF SYMBOLS VII
1. GENERAL INTRODUCTION AND OBJECTIVES OF THE DISSERTATION 1
2. CARBON FIBER REINFORCED MATAL MATRIX COMPOSITES (CF/MMCS) 3
2.1. COMPONENTS OF FIBER REINFORCED METAL MATRIX COMPOSITES (CF/MMCS)
2.1.1. ALUMINUM ALLOYS (AL-ALLOYS)
2.1.2. MAGNESIUM ALLOYS (MG-ALLOYS)
2.1.3. CARBON FIBER
2.1.3.1. PROPERTIES, STRUCTURES AND TYPES
2.1.3.2. CARBON FIBER PRODUCTION PROCESS
2.2. FABRICATION OF
CF/MMCS
BY LIQUID METAL INFILTRATION
2.2.1. GAS PRESSURE INFILTRATION (GPI)
2.2.2. DIRECT SQUEEZE CASTING 10
2.2.3. HIGH PRESSURE DIE CASTING (HPDC) 11
2.3. WETTING BETWEEN FIBERS AND METAL MATRIX 11
2.3.1. THE ROLE OF WETTING 11
2.3.2. TAILORING OF FIBER-MATRIX INTERFACE IN
CF/MMCS
12
2.4. STATE OF THE ART CARBON FIBER COATINGS FOR THE USE IN METAL
MATRIX COMPOSITES (MMCS) 14
3. DEPOSITION METHODS FOR FIBER COATING 18
3.1. SOL-GEL TECHNIQUE 18
3.2. MOLTEN SALT TECHNIQUE 18
3.3. PHYSICAL VAPOR DEPOSITION (PVD) 18
3.4. ELECTROPLATING 19
3.5. ELECTROLESS PLATING 19
3.6. CHEMICAL VAPOR DEPOSITION (CVD) 20
3.6.1. GENERAL INFORMATION 20
3.6.2. THERMODYNAMICS OF CVD 22
3.6.3. DEPOSITION MECHANISM AND MASS TRANSPORT PHENOMENA 23
3.6.4. KINETICS OF CVD 26
3.6.5. THIN FILM GROWTH 29
3.7. ATOMIC LAYER DEPOSITION (ALD) 30
3.7.1. GENERAL INFORMATION 30
3.7.2. ALD PROCESS WINDOW 31
3.7.3. ALD REACTOR TYPES AND PRECURSOR REQUIREMENTS 32
4. BASICS AND STATE OF THE ART OF TIN,
AI2O3
AND TIS
2
/TIN 34
4.1. CVD OF TITANIUM NITRIDE (TIN) 34
4.2. ALD OF ALUMINUM OXIDE
(AI2O3)
37
4.3. CVD OF TITANIUM DISULFIDE (T
1
S
2
) 40
(0(0000)0 AI-TW-^
5. EXPERIMENTAL WORK
42
5.1. COATING OF CARBON FIBERS 42
5.1.1. CVD OF TITANIUM NITRIDE (TIN) 42
5.1.2. CVD OF TITANIUM DISULFIDE (TIS2) AND DOUBLE LAYER TIS2/TIN 43
5.1.3. A L D O FA H O S 43
5.2. MATERIALS 44
5.3. COMPOSITE MANUFACTURE BY GAS PRESSURE INFILTRATION (GPI) 45
5.4. ANALYTICAL METHODS 46
5.4.1. SCANNING ELECTRON MICROSCOPY (SEM) 46
5.4.2. TRANSMISSION ELECTRON MICROSCOPY (TEM) 47
5.4.3. X-RAY PHOTOELECTRON SPECTROSCOPY (XPS) 48
5.4.4. THERMOGRAVIMETRIC ANALYSES (TGA) 49
5.4.5. X-RAY DIFFRACTION ANALYSIS (XRD) 49
5.4.6. SESSILE DROP TEST 50
5.4.7. TENSILE STRENGTH OF COATED FIBERS 51
6. RESULT AND DISCUSSION 53
6.1. THERMAL TREATMENT OF CARBON FIBERS PRIOR TO DEPOSITION 53
6.2. CVD OF TITANIUM NITRIDE (TIN) 54
6.2.1. STRUCTURE, COMPOSITION AND THICKNESS HOMOGENEITY OF TIN COATINGS
55
6.2.2. OXIDATION BEHAVIOR AND TENSILE STRENGTH OF UNCOATED AND COATED
FIBERS 59
6.2.3. WETTABILITY TEST AND INTERFACE ANALYSIS OF AI/TIN/CGR 60
6.3. ALD OF ALUMINUM OXIDE (AL203) 62
6.3.1. STRUCTURE, COMPOSITION AND THICKNESS HOMOGENEITY OF ALUMINA
COATINGS 63
6.3.2. OXIDATION BEHAVIOR AND TENSILE STRENGTH OF AI203-COATED
HM-/HT-FIBERS 66
6.3.2.1 HTS40 FIBERS (HIGH TENACITY) 66
6.3.2.2 M40J FIBERS (HIGH MODULUS) 67
6.3.3. WETTABILITY TEST OF AI203-COATED GRAPHITE WITH CP-AI AND ALSICU
(226D) 68
6.4. CVD OF TITANIUM DISULFIDE (TIS2) AND TIS2/TIN DOUBLE COATINGS 69
6.4.1. THERMODYNAMIC ANALYSIS OF THE CVD SYSTEM TI-S-CI-H-AR 69
6.4.2. STRUCTURE, COMPOSITION AND DEPOSITION RATE OF TIS2 COATING
DEPOSITED ON PLANAR
GRAPHITE SUBSTRATE 71
6.4.3. STRUCTURE AND THICKNESS HOMOGENEITY OF TIS2 SINGLE COATINGS AND
TISX/TIN
DOUBLE COATINGS ON CARBON FIBER FABRICS 80
6.4.4. OXIDATION BEHAVIOR AND TENSILE STRENGTH OF UNCOATED AND COATED
FIBERS 83
6.5. MMC BY INFILTRATION OF UNCOATED AND COATED CARBON FIBER FABRICS 85
6.5.1. INFILTRATION OF TIN-COATED 3D-HTS-TEXTILE PREFORM WITH 226D BY
GPI METHOD 85
6.5.2. INFILTRATION OF TIN-COATED 2D/3D-HTS-TEXTILE PREFORM WITH AZ91 BY
GPI METHOD 89
6.5.3. INFILTRATION OF UNCOATED- AND AI203-COATED 2D-HM-TEXTILE PREFORM
WITH
226D BY GPI METHOD 93
6.5.4. INFILTRATION OF UNCOATED- AND AI203-COATED 2D-HM-TEXTILE PREFORM
WITH
239D BY GPI METHOD 98
6.5.5. INFILTRATION OF UNCOATED- AND AI203-COATED 2D -H TS TEXTILE
PREFORM WITH
AZ91 BY GPI METHOD 101
6.5.6. INFILTRATION BEHAVIOR OF TIN-AND AI203-COATED 3D-HTS-TEXTILE
PREFORMS WITH
226D BY HPDC METHOD 105
7. SUMMARY AND OUTLOOK 106
8. DIRECTORIES 110
8.1. REFERENCES 110
8.2. LIST OF FIGURES 123
8.3. LIST OF TABLES 130
8.4. LIST OF PUBLICATIONS RELATED WITH THIS WORK 131 |
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| discipline | Maschinenbau / Maschinenwesen Werkstoffwissenschaften / Fertigungstechnik |
| discipline_str_mv | Maschinenbau / Maschinenwesen Werkstoffwissenschaften / Fertigungstechnik |
| format | Thesis Book |
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| index_date | 2024-07-03T17:05:37Z |
| indexdate | 2024-07-10T09:06:41Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-032648408 |
| oclc_num | 1189070762 |
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| owner_facet | DE-83 |
| physical | VIII, 131 Seiten Illustrationen, Diagramme 21 cm |
| publishDate | 2016 |
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| spelling | Abidin, Alfaferi Zainal 1975- Verfasser (DE-588)1173735011 aut Materialwissenschaftliche Untersuchungen zur Oberflächenmodifizierung von Kohlenstofffasern in faserverstärkten Metallkompositen vorgelegt von Alfaferi Zainal Abidin Dresden Oktober 2016 VIII, 131 Seiten Illustrationen, Diagramme 21 cm txt rdacontent n rdamedia nc rdacarrier Dissertation Technische Universität Dresden 2017 Modifizierung (DE-588)4299539-5 gnd rswk-swf Oberfläche (DE-588)4042907-6 gnd rswk-swf Kohlenstofffaser (DE-588)4128150-0 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Kohlenstofffaser (DE-588)4128150-0 s Modifizierung (DE-588)4299539-5 s Oberfläche (DE-588)4042907-6 s DE-604 B:DE-101 application/pdf http://d-nb.info/1173353380/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032648408&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Abidin, Alfaferi Zainal 1975- Materialwissenschaftliche Untersuchungen zur Oberflächenmodifizierung von Kohlenstofffasern in faserverstärkten Metallkompositen Modifizierung (DE-588)4299539-5 gnd Oberfläche (DE-588)4042907-6 gnd Kohlenstofffaser (DE-588)4128150-0 gnd |
| subject_GND | (DE-588)4299539-5 (DE-588)4042907-6 (DE-588)4128150-0 (DE-588)4113937-9 |
| title | Materialwissenschaftliche Untersuchungen zur Oberflächenmodifizierung von Kohlenstofffasern in faserverstärkten Metallkompositen |
| title_auth | Materialwissenschaftliche Untersuchungen zur Oberflächenmodifizierung von Kohlenstofffasern in faserverstärkten Metallkompositen |
| title_exact_search | Materialwissenschaftliche Untersuchungen zur Oberflächenmodifizierung von Kohlenstofffasern in faserverstärkten Metallkompositen |
| title_exact_search_txtP | Materialwissenschaftliche Untersuchungen zur Oberflächenmodifizierung von Kohlenstofffasern in faserverstärkten Metallkompositen |
| title_full | Materialwissenschaftliche Untersuchungen zur Oberflächenmodifizierung von Kohlenstofffasern in faserverstärkten Metallkompositen vorgelegt von Alfaferi Zainal Abidin |
| title_fullStr | Materialwissenschaftliche Untersuchungen zur Oberflächenmodifizierung von Kohlenstofffasern in faserverstärkten Metallkompositen vorgelegt von Alfaferi Zainal Abidin |
| title_full_unstemmed | Materialwissenschaftliche Untersuchungen zur Oberflächenmodifizierung von Kohlenstofffasern in faserverstärkten Metallkompositen vorgelegt von Alfaferi Zainal Abidin |
| title_short | Materialwissenschaftliche Untersuchungen zur Oberflächenmodifizierung von Kohlenstofffasern in faserverstärkten Metallkompositen |
| title_sort | materialwissenschaftliche untersuchungen zur oberflachenmodifizierung von kohlenstofffasern in faserverstarkten metallkompositen |
| topic | Modifizierung (DE-588)4299539-5 gnd Oberfläche (DE-588)4042907-6 gnd Kohlenstofffaser (DE-588)4128150-0 gnd |
| topic_facet | Modifizierung Oberfläche Kohlenstofffaser Hochschulschrift |
| url | http://d-nb.info/1173353380/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032648408&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT abidinalfaferizainal materialwissenschaftlicheuntersuchungenzuroberflachenmodifizierungvonkohlenstofffaserninfaserverstarktenmetallkompositen |
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Inhaltsverzeichnis